Abstract
In this paper, we present the microwave-assisted synthesis and characterization of alkaline nanomaterials for the preservation of cultural heritage. Calcium and barium hydroxide nanomaterials suspended in aqueous as well as alcoholic medium were applied on different samples to check their effectiveness. The effect of treatment was measured using pH value and alkaline reserve test. The alkaline reserve test results indicate improvement in the alkaline buffer with significant reduction in acidity of the papers and improvement in pH value of the surfaces. Ethanol was found as best solvent on the basis of suspension of nanoparticles, pH value and ease of application through spray gun. Accelerated ageing test revealed that the reinforcement effect of these nanomaterials persisted throughout the ageing. All the results converged in individuating these nanometric particles as an innovative, completely compatible, and efficient material for the consolidation of old and new paper surfaces.
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References
Schmude, I.G.: Can of Paper Deterioration, Library Collections Survive? The Problem The Australian Library Journal 33(1) (February 1984)
Barrows, W.J.: Permanence/Durability of the Book, Physical and Chemical Properties of Book Papers, vol. VII, pp. 1507–1949. Research Laboratory, Inc. (1974)
Ott, Spurlin, and Grafflin, pp. 99-191 (1954)
Church, R.W, pp. 14-16 (1959)
Barrow, pp. 6-7 (1965)
Polymer Degradation and Stability 91, 3448-3455 (2006)
Ipert, S., Rousset, E., Cheradame, H.: International Journal for the Preservation of Library and Archival Material 26, 250-264 (2005)
Journal of Cultural Heritage 7, 110–115 (2006)
Salvadori, B., Dei, L.: Synthesis of Ca(OH)2 nanoparticles from diols. Langmuir 17, 2371–2374 (2001)
Giorgi, R., Bozzi, C., Dei, L.G., Gabbiani, C., Ninham, B.W., Baglioni, P.: Langmuir 21, 8495-8501 (2005)
Giorgi, R., Chelazzi, D., Langmuir, P.B.: 21, pp. 10743-10748 (2005)
Ambrosi, M., Dei, L., Giorgi, R., Neto, C., Baglioni, P.: Colloidal particles of Ca(OH)2: properties and applications to restoration of frescoes. Langmuir 17, 4251–4255 (2001)
ANSI NISO Standard Z39.48-1992R2002
Teygeler, R.: Preserving paper: Recent advances. In: Feather, J. (ed.) Managing preservation for libraries and archives: Current practice and future development, vol. 89. Ashgate, Burlington (2004) ISBN 0-7546-0705-4
Dahlo, R.: The Rationale of permanent Paper. In: Manning, W., Kremp, V. (eds.) IFLA Publications 91: A Reader in preservation and conservation, vol. 59. K. G. Saur, Munchen (2000) ISBN 3-598-21817-6.
ASTM D 3290-00, Standard Specification for Bond and Ledger Papers for Permanent Records, section 3.2.3.2 and Appendix X1
ASTM D 4988, Standard Test Method for Determination of Alkalinity of Paper as Calcium Carbonate (Alkaline Reserve of Paper) (1996)
Determination of the Alkali Reserve according to ISO 10716: for the paper (1994)
Hydrogen ion concentration (pH) of paper extracts (cold extraction method), Test Method T 509 om-11
Technical Association of the Pulp and Paper Industry. TAPPI Standard Test T435-52; Hydrogen Ion Content (pH). Technical Association of the Pulp and Paper Industry, New York (1952)
A hot water extraction method is described in TAPPI T 435, Hydrogen Ion Concentration (pH) of Paper Extracts (Hot Extraction Method)
Lundeen, G.W.: Preservation of paper based materials: Present and future research and developments in the paper industry. In: Henderson, K.L., Henderson, W.T. (eds.) Conserving and preserving library materials (Papers presented at the Allerton Park Institute, November 15–18, pp. 73–88 (1981), http://hdl.handle.net/2142/459 , (retrieved)
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Saoud, K.M., Ibala, I., El Ladki, D., Ezzeldeen, O., Saeed, S. (2014). Microwave Assisted Preparation of Calcium Hydroxide and Barium Hydroxide Nanoparticles and Their Application for Conservation of Cultural Heritage. In: Ioannides, M., Magnenat-Thalmann, N., Fink, E., Žarnić, R., Yen, AY., Quak, E. (eds) Digital Heritage. Progress in Cultural Heritage: Documentation, Preservation, and Protection. EuroMed 2014. Lecture Notes in Computer Science, vol 8740. Springer, Cham. https://doi.org/10.1007/978-3-319-13695-0_33
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DOI: https://doi.org/10.1007/978-3-319-13695-0_33
Publisher Name: Springer, Cham
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